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GmbH & Co. KG
Hirtenrasen 64
D-37318 Lindewerra
Phone: +49 36087 976-0
Fax +49 36087 976-22
 
 
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Distillation und Extraction plants

   
Plant: 4-Reactor-Crystallizer Unit
   
Main Apparatus: 4x Triple Jacketed Reactors (2x 5l and 2x 10l), 1x Condenser for each Reactor, Liquid Feed, Vacuum-System with 2 lines
Materials: Glass, PTFE, PFA
Vacuum: 10 mbar abs.
Cooling: -30 to 20°C
Thermostate: -40 to 130°C
Control System: Siemens S7, PC with Simatic WinCC, recipe control
   
Plant: Distillation Plant
   
Column: ø 30 packing column
Materials: Stainless Steel 1.4571
Feed: 2 l/h
Product Vessels: 10 l
Reflux Divider: electropneumatic
Cooling: thermostat
Temperature: max. 350 °C
Control System: Siemens S7 and Simatic WinCC
   
Plant: Glass plant with Sulzer Packing 
   
Column: DN 40, vacuum jacket, mirrored
Materials: Glass, PTFE, PVDF
Evaporator:
1,5 kW Quarz glass, horizontal with stirrer and circulation loop
Phase Separator: Glass, with adjustable overflow
Reflux Divider:

Funnel with magnet

Feed: 2 l/h, Dosing by gravity, heated
Product Vessel: 3 x 5 l, with level measurement
Vacuum: 2,3 m³/h, 1000 to 12 mbar, geregelt
Cooling: via Thermostat
Control System: Siemens S7 and PC with Simatic WinCC
   
Plant: Glass Plant with Sieve Trays
   
Column: DN 30 mirrored, sieve trays
Materials: Glas, PTFE, PVDF 
Evaporator: Round flask, 0,7 kW electrical heating jacket
Phase Separator: Glass, with adjustable outlet
Reflux Divider:

Funnel with magnet

Feed: 2 l/h,  dosing by gravity, heated
Product Vessels: 3 x 3 l, round flask
Vacuum: 2,3 m³/h, 1000 to 12 mbar, speed controlled
Cooling: with cooling water
Control System: Siemens S7 with PC and Simatic WinCC
   
Plant: Vacuum and Pressure Distillation with Sulzer Packs
   
Column: DN 50 insulated, Sulzer Packs
Materials: Stainless steel 1.4571 (SS 316 Ti and 316 L)
Evaporator:
Stirred vessel with level measurement at the side, electrical heating 1.5 kW.
Phase Separator: Stainless Steel with 2 sight glasses for the Adjustment of Outflows
Reflux Divider:

Funnel with magnet

Feed: 3 x Dosing, 6, 2, und 1 l/h, feed on balance
Product Vessels: 3 x 1 l intermediate vessel on balance, 10 l product storage
Vacuum: 1000 to 8 mbar, controlled, redundant with 2 pumps.
Cooling: with cooling water, Condenser with 2 stages, second stage with a cooling machine, deep temperature trap with -50 °C cooling machine.
Control System: Siemens S7 with PC and Simatic WinCC
   
Plant: 2-Stage Evaporator
   
Column: none
Materials: Glass, stainless steel, PTFE, PVDF
Evaporator: 1. Stage: electrical, 6 kW
2. Stage: steam condenser from stage 1
Feed: Dosing pump, pulse controlled
Product Vessels: 2 x 10 l Product vessels
Vacuum: 1000 to 12 mbar, controlled
Cooling: with cooling water
Control System: Siemens S7 with PC and Simatic ProTool Pro
   
Plant: Pulsing Extraction und Distillation
   
Column: Extraction Glass, DN 40 with 42 stainless steel sieve trays
Distillation Glass, DN 40 with Raschig Rings
Materials: Glass, stainless steel, PTFE,  PVDF
Pulsator: Diaphragm pump, modified, Volume adjustable
Feed: 2 Dosing pumps, pulse controlled
Product Vessels: 2 x 15 l Collection vessels + 2 l for bottom product
Reflux Divider:

Funnel with magnet

Cooling: with cooling water
Control System: Single devices for reflux divider, temperature controller, pulse frequency control
   
Plant: Distillation Plant
   
Column: DN 40, Sulzer packings
Materials: Glass, PTFE
Feed: 2 kg/h
Product Vessels: 5 l Glass vessel
Reflux Divider:

Funnel type

Cooling: cooling maschine, - 10 °C
Control System: Eurotherm