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| AP-Miniplant |
| GmbH & Co. KG |
| Hirtenrasen 64 |
| D-37318 Lindewerra |
| Phone: +49 36087 976-0 |
| Fax +49 36087 976-22 |
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German | English | Russian | Chinese | | |
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Distillation und Extraction plants
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| Plant: |
4-Reactor-Crystallizer Unit |
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| Main Apparatus: |
4x Triple Jacketed Reactors (2x 5l and 2x 10l), 1x Condenser for each Reactor, Liquid Feed, Vacuum-System with 2 lines |
| Materials: |
Glass, PTFE, PFA |
| Vacuum: |
10 mbar abs. |
| Cooling: |
-30 to 20°C |
| Thermostate: |
-40 to 130°C |
| Control System: |
Siemens S7, PC with Simatic WinCC, recipe control | |
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| Plant: |
Distillation Plant |
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| Column: |
ø 30 packing column |
| Materials: |
Stainless Steel 1.4571 |
| Feed: |
2 l/h |
| Product Vessels: |
10 l |
| Reflux Divider: |
electropneumatic |
| Cooling: |
thermostat |
| Temperature: |
max. 350 °C |
| Control System: |
Siemens S7 and Simatic WinCC | |
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| Plant: |
Glass plant with Sulzer Packing |
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| Column: |
DN 40, vacuum jacket, mirrored |
| Materials: |
Glass, PTFE, PVDF |
Evaporator:
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1,5 kW Quarz glass, horizontal with stirrer and circulation loop |
| Phase Separator: |
Glass, with adjustable overflow |
| Reflux Divider: |
Funnel with magnet |
| Feed: |
2 l/h, Dosing by gravity, heated |
| Product Vessel: |
3 x 5 l, with level measurement |
| Vacuum: |
2,3 m³/h, 1000 to 12 mbar, geregelt |
| Cooling: |
via Thermostat |
| Control System: |
Siemens S7 and PC with Simatic WinCC | |
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| Plant: |
Glass Plant with Sieve Trays |
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| Column: |
DN 30 mirrored, sieve trays |
| Materials: |
Glas, PTFE, PVDF |
| Evaporator: |
Round flask, 0,7 kW electrical heating jacket |
| Phase Separator: |
Glass, with adjustable outlet |
| Reflux Divider: |
Funnel with magnet |
| Feed: |
2 l/h, dosing by gravity, heated |
| Product Vessels: |
3 x 3 l, round flask |
| Vacuum: |
2,3 m³/h, 1000 to 12 mbar, speed controlled |
| Cooling: |
with cooling water |
| Control System: |
Siemens S7 with PC and Simatic WinCC | |
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| Plant: |
Vacuum and Pressure Distillation with Sulzer Packs |
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| Column: |
DN 50 insulated, Sulzer Packs |
| Materials: |
Stainless steel 1.4571 (SS 316 Ti and 316 L) |
Evaporator:
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Stirred vessel with level measurement at the side, electrical heating 1.5 kW. |
| Phase Separator: |
Stainless Steel with 2 sight glasses for the Adjustment of Outflows |
| Reflux Divider: |
Funnel with magnet |
| Feed: |
3 x Dosing, 6, 2, und 1 l/h, feed on balance |
| Product Vessels: |
3 x 1 l intermediate vessel on balance, 10 l product storage |
| Vacuum: |
1000 to 8 mbar, controlled, redundant with 2 pumps. |
| Cooling: |
with cooling water, Condenser with 2 stages, second stage with a cooling machine, deep temperature trap with -50 °C cooling machine. |
| Control System: |
Siemens S7 with PC and Simatic WinCC | |
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| Plant: |
2-Stage Evaporator |
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| Column: |
none |
| Materials: |
Glass, stainless steel, PTFE, PVDF |
| Evaporator: |
1. Stage: electrical, 6 kW 2. Stage: steam condenser from stage 1 |
| Feed: |
Dosing pump, pulse controlled |
| Product Vessels: |
2 x 10 l Product vessels |
| Vacuum: |
1000 to 12 mbar, controlled |
| Cooling: |
with cooling water |
| Control System: |
Siemens S7 with PC and Simatic ProTool Pro | |
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| Plant: |
Pulsing Extraction und Distillation |
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| Column: |
Extraction Glass, DN 40 with 42 stainless steel sieve trays Distillation Glass, DN 40 with Raschig Rings |
| Materials: |
Glass, stainless steel, PTFE, PVDF |
| Pulsator: |
Diaphragm pump, modified, Volume adjustable |
| Feed: |
2 Dosing pumps, pulse controlled |
| Product Vessels: |
2 x 15 l Collection vessels + 2 l for bottom product |
| Reflux Divider: |
Funnel with magnet |
| Cooling: |
with cooling water |
| Control System: |
Single devices for reflux divider, temperature controller, pulse frequency control | |
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| Plant: |
Distillation Plant |
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| Column: |
DN 40, Sulzer packings |
| Materials: |
Glass, PTFE |
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| Feed: |
2 kg/h |
| Product Vessels: |
5 l Glass vessel |
| Reflux Divider: |
Funnel type |
| Cooling: |
cooling maschine, - 10 °C |
| Control System: |
Eurotherm | |
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